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Beilstein J. Org. Chem. 2017, 13, 755–761, doi:10.3762/bjoc.13.74
Graphical Abstract
Figure 1: Targeted compounds.
Figure 2: Retrosynthesis of compound 1.
Scheme 1: Synthesis of 5-(2’-C-methyl-β-D-ribofuranosyl)-1,2,3-triazole-4-carboxamide (2).
Scheme 2: Synthesis of the 2’-keto derivatives 12a/12b.
Figure 3: X-ray spectrum of compound 10b.
Figure 4: Structural study of isomeric compounds 13.
Scheme 3: Fluorination of ethyl 1-benzyl-4-(2’-C-methyl-3’,5’-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribof...
Scheme 4: Synthesis of 5-(2’-deoxy-2’-fluoro-2’-methyl-β-D-ribofuranosyl)-1,2,3-triazole-4-carboxamide (3).